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Re: ORGLIST: grignard

From: Vedran Hasimbegovic <vedran.hasimbegovic>
Subject: Re: ORGLIST: grignard
Date: Wed, 14 Mar 2012 10:42:12 +0100
Hi there,

Titration can be used, there is a forum discussion on this: http://www.chemicalforums.com/index.php?topic=17690.0

Hope it helps

//Vedran

On Wed, Mar 14, 2012 at 3:57 AM, Shailesh kumar Pansuriya <shreejisky> wrote:

Surprised by quick email. Sir. I am preparing Methyl Magnesium Iodide. 30 g Mg + 180 g Methyl Iodide + 500 ml Diethyl Ether and make grig.   As i need the grig free from water, alcohol, aldehyde, free from unreacted Mg. but how could i check the quality of grig.?
Really very very Thanks for reply

On Mar 14, 2012 1:11 AM, "Guido de Silvestri" <gde> wrote:
Dear Shailesh....

What exactly is the problem you are having with the synthesis?


-----Original Message-----
From: orglist-everybody
[mailto:orglist-everybody] On Behalf Of Shailesh kumar
Pansuriya
Sent: Tuesday, March 13, 2012 3:08 AM
To: OrgList
Subject: ORGLIST: grignard

hi, any one who help me to solve the problems in grignard synthesis?





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