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RE: ORGLIST: grignard

From: Shailesh kumar Pansuriya <shreejisky>
Subject: RE: ORGLIST: grignard
Date: Wed, 14 Mar 2012 08:27:02 +0530

Surprised by quick email. Sir. I am preparing Methyl Magnesium Iodide. 30 g Mg + 180 g Methyl Iodide + 500 ml Diethyl Ether and make grig.   As i need the grig free from water, alcohol, aldehyde, free from unreacted Mg. but how could i check the quality of grig.?
Really very very Thanks for reply

On Mar 14, 2012 1:11 AM, "Guido de Silvestri" <gde> wrote:
Dear Shailesh....

What exactly is the problem you are having with the synthesis?

-----Original Message-----
From: orglist-everybody
[mailto:orglist-everybody] On Behalf Of Shailesh kumar
Sent: Tuesday, March 13, 2012 3:08 AM
To: OrgList
Subject: ORGLIST: grignard

hi, any one who help me to solve the problems in grignard synthesis?

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